TÜRKÇE
ENGLISH
Information
| Unit | FACULTY OF PHARMACY |
| PHARMACY PR. | |
| Code | ECF209 |
| Name | Analytical Chemistry Laboratory II |
| Term | 2017-2018 Academic Year |
| Semester | 3. Semester |
| Duration (T+A) | 0-3 (T-A) (17 Week) |
| ECTS | 2 ECTS |
| National Credit | 1.5 National Credit |
| Teaching Language | Türkçe |
| Level | Lisans Dersi |
| Type | Normal |
| Label | C Compulsory |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Doç. Dr. SABRİYE AYDINOĞLU MARINELLI |
| Course Instructor |
Doç. Dr. SABRİYE AYDINOĞLU MARINELLI
(Güz)
(A Group)
(Ins. in Charge)
Doç. Dr. SABRİYE AYDINOĞLU MARINELLI (Güz) (B Group) (Ins. in Charge) |
Course Goal / Objective
The student is expected to become familiar with the instrumental analysis methods, their basis and potential use.
Course Content
Elektrokimyasal, Spektroskimyasal ve kromatografik analiz yöntemlerinin ve validasyon parametrelerinin öğrenilmesi
Course Precondition
Resources
Notes
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | Explain the principles of potentiometric titration and use it to calculate the equilibrium constants of a polyprotic acid or base. |
| LO02 | Uses UV-Visible spectroscopy in the analysis of mixtures. |
| LO03 | Performs Qualitative Analysis Using Thin Layer Chromatography. |
| LO04 | Performs Quantitative Analysis with Refractometry |
| LO05 | Applies derivative spectroscopy in the quantitative analysis of pharmaceutical mixtures. |
| LO06 | Performs quantitative analysis by atomic absorption spectrophotometry. |
| LO07 | Applies column chromatography. |
| LO08 | Explains the basic principles of high performance liquid chromatography. |
| LO09 | Gain the ability to apply the information learned about conductivity titration in complex acid-base systems. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Have sufficient knowledge in pharmaceutical field and develop the knowledge. | 3 |
| PLO02 | Bilgi - Kuramsal, Olgusal | Comprehends professional knowledge with ethical responsibility through current laws and legislation. | 2 |
| PLO03 | Beceriler - Bilişsel, Uygulamalı | Provides consultancy service to patients, community and health care personnel and evaluates advanced knowledge and skills with a critical approach. | |
| PLO04 | Beceriler - Bilişsel, Uygulamalı | Possessing the knowledge of historical and current developments in the field of Pharmacy, monitoring, evaluation and application of scientific and evidence-based data, and adopting lifelong learning. | 4 |
| PLO05 | Beceriler - Bilişsel, Uygulamalı | Have the knowledge and skills to help provide patient-oriented pharmacy applications and individualized pharmaceutical care by learning the basics of Clinical Pharmacy, | |
| PLO06 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | Takes a role in the evaluation and analysis of the events and cases related to the development of pharmacy profession and education. | |
| PLO07 | Yetkinlikler - Öğrenme Yetkinliği | Integrates and develops professional knowledge via different disciplines and uses the acquired knowledge to improve the health level and quality of life of the community. | 3 |
| PLO08 | Yetkinlikler - Öğrenme Yetkinliği | Use effectively the concepts and applications of basic sciences and basic medical sciences in the field of medicine and pharmacy and update the information. | 4 |
| PLO09 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Communicates effectively in writing and speaking. | 3 |
| PLO10 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Practices the profession in accordance with Atatürk's principles and reforms, equipped with universal knowledge, uses Turkish correctly and knows at least one foreign language. | |
| PLO11 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Be an example to society withexternal appearance, demeanor, attitude and behavior for the other professionals and society and with professional identity | |
| PLO12 | Yetkinlikler - Alana Özgü Yetkinlik | Have knowledge about health policies and health economics, pharmacy management and define the problems in pharmaceutical field. | |
| PLO13 | Yetkinlikler - Alana Özgü Yetkinlik | Interprets information about current health and treatment problems and attends meeting on related matters . Plays an active role in community health. | |
| PLO14 | Yetkinlikler - Alana Özgü Yetkinlik | Acquires basic information about diseases, makes decisions about the drugs used in treatment in accordance with rational drug use. |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Introduction of spectroscopic, chromatographic and electrochemical analysis methods | Quiz and Report | |
| 2 | Conductivity analysis of strong and weak acids | Quiz and Report | |
| 3 | Potentiometric titration of polyprotic acids or bases | Quiz and Report | |
| 4 | Spectrophotometric determination of two-component mixtures | Quiz and Report | |
| 5 | Analysis of binary mixtures by differential UV spectrophotometry | Quiz and Report | |
| 6 | Determination of complex formulas and stability constants by spectrophotometric method | Quiz and Report | |
| 7 | Mixture analysis by spectrophotometric titration | Quiz and Report | |
| 8 | Mid-Term Exam | Written Exam | |
| 9 | Introduction to Validation | Quiz and Report | |
| 10 | Qualitative analysis of drugs by thin layer chromatography | Quiz and Report | |
| 11 | Separation of indicator mixtures by column chromatography | Quiz and Report | |
| 12 | Quantitative analysis by high performance liquid chromatography | Quiz and Report | |
| 13 | Cation analysis by atomic absorption spectroscopy | Quiz and Report | |
| 14 | Kinetic Determination of Trace Copper | Quiz and Report | |
| 15 | Validation Study | Presentation | |
| 16 | Term Exams | Written exam | |
| 17 | Term Exams | Written exam |
Assessment (Exam) Methods and Criteria
| Assessment Type | Midterm / Year Impact | End of Term / End of Year Impact |
|---|---|---|
| 1. Midterm Exam | 35 | 14 |
| 1. Short Exam | 35 | 14 |
| 1. Homework | 30 | 12 |
| General Assessment | ||
| Midterm / Year Total | 100 | 40 |
| 1. Final Exam | - | 60 |
| Grand Total | - | 100 |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 1 | 14 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 2 | 28 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 3 | 3 |
| Final Exam | 1 | 9 | 9 |
| Total Workload (Hour) | 54 | ||
| Total Workload / 25 (h) | 2,16 | ||
| ECTS | 2 ECTS | ||