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Information
| Unit | FACULTY OF PHARMACY |
| PHARMACY PR. | |
| Code | ECF306 |
| Name | Pharmaceutical Chemistry Laboratory III |
| Term | 2018-2019 Academic Year |
| Semester | 6. Semester |
| Duration (T+A) | 0-3 (T-A) (17 Week) |
| ECTS | 2 ECTS |
| National Credit | 1.5 National Credit |
| Teaching Language | Türkçe |
| Level | Lisans Dersi |
| Type | Normal |
| Label | C Compulsory |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Dr. Öğr. Üyesi ÖZDEN TARI |
| Course Instructor |
Dr. Öğr. Üyesi ÖZDEN TARI
(Bahar)
(A Group)
(Ins. in Charge)
Dr. Öğr. Üyesi ÖZDEN TARI (Bahar) (B Group) (Ins. in Charge) |
Course Goal / Objective
The purpose of this course is to give the principles and applications of the instrumental techniques such as ultraviolet, infrared, nuclear magnetic resonance and mass spectroscopic used in qualitative analysis and structural elucidation of drugs and application of drugs synthesis.
Course Content
The course contains the knowledge, principles and applications of the instrumental techniques such as ultraviolet, infrared, nuclear magnetic resonance, mass spectroscopic and elementary analysis used in qualitative analysis and structural elucidation of drugs. Literature studies are conducted on the synthesis and analysis of some drugs.
Course Precondition
Resources
Notes
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | The student who completes this course learn instrumental techniques such as UV, IR, NMR and mass used in structural elucidation of organic compounds |
| LO02 | The student who completes this course the ability of structural elucidation of the molecule using all spectral data at the same time. |
| LO03 | The student who completes this course learn how to reach to the structure of unknown compound by means of spectral data. |
| LO04 | The student who completes this course learn knowledge and application skills about the synthesis of selected drug molecules. |
| LO05 | The student who completes this course learn how to reach to the information of analysis and mechanism of action of the compounds synthesized using databases and scientific resources. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Have sufficient knowledge in pharmaceutical field and develop the knowledge. | |
| PLO02 | Bilgi - Kuramsal, Olgusal | Comprehends professional knowledge with ethical responsibility through current laws and legislation. | 3 |
| PLO03 | Beceriler - Bilişsel, Uygulamalı | Provides consultancy service to patients, community and health care personnel and evaluates advanced knowledge and skills with a critical approach. | |
| PLO04 | Beceriler - Bilişsel, Uygulamalı | Possessing the knowledge of historical and current developments in the field of Pharmacy, monitoring, evaluation and application of scientific and evidence-based data, and adopting lifelong learning. | 1 |
| PLO05 | Beceriler - Bilişsel, Uygulamalı | Have the knowledge and skills to help provide patient-oriented pharmacy applications and individualized pharmaceutical care by learning the basics of Clinical Pharmacy, | 2 |
| PLO06 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | Takes a role in the evaluation and analysis of the events and cases related to the development of pharmacy profession and education. | 2 |
| PLO07 | Yetkinlikler - Öğrenme Yetkinliği | Integrates and develops professional knowledge via different disciplines and uses the acquired knowledge to improve the health level and quality of life of the community. | 3 |
| PLO08 | Yetkinlikler - Öğrenme Yetkinliği | Use effectively the concepts and applications of basic sciences and basic medical sciences in the field of medicine and pharmacy and update the information. | |
| PLO09 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Communicates effectively in writing and speaking. | |
| PLO10 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Practices the profession in accordance with Atatürk's principles and reforms, equipped with universal knowledge, uses Turkish correctly and knows at least one foreign language. | |
| PLO11 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Be an example to society withexternal appearance, demeanor, attitude and behavior for the other professionals and society and with professional identity | |
| PLO12 | Yetkinlikler - Alana Özgü Yetkinlik | Have knowledge about health policies and health economics, pharmacy management and define the problems in pharmaceutical field. | |
| PLO13 | Yetkinlikler - Alana Özgü Yetkinlik | Interprets information about current health and treatment problems and attends meeting on related matters . Plays an active role in community health. | |
| PLO14 | Yetkinlikler - Alana Özgü Yetkinlik | Acquires basic information about diseases, makes decisions about the drugs used in treatment in accordance with rational drug use. | 2 |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Demonstration (Elemental Analysis) | Textbooks, Laboratory sheet | |
| 2 | Demonstration (Introduction to spectroscopy and UV) | Textbooks, Laboratory sheet | |
| 3 | IR spectrometry | Textbooks, Laboratory sheet | |
| 4 | 1H-NMR spectrometry | Textbooks, Laboratory sheet | |
| 5 | 13C-NMR spectrometry | Textbooks, Laboratory sheet | |
| 6 | Mass spectrometry | Textbooks, Laboratory sheet | |
| 7 | Investigation of the spectrum of unknown 1th group compound | Textbooks, Laboratory sheet | |
| 8 | Mid-Term Exam | Textbooks, Laboratory sheet | |
| 9 | Investigation of the spectrum of unknown 2nd group compound | Textbooks, Laboratory sheet | |
| 10 | Benzimidazole derivative drug synthesis | Textbooks, Laboratory sheet | |
| 11 | İsoniazide synthesis | Textbooks, Laboratory sheet | |
| 12 | Paracetamol synthesis | Textbooks, Laboratory sheet | |
| 13 | Homework and Discussion | Textbooks, Laboratory sheet | |
| 14 | Homework and Discussion-2 | Textbooks, Laboratory sheet | |
| 15 | Homework and Discussion-3 | Textbooks, Laboratory sheet | |
| 16 | Term Exams | Textbooks, Laboratory sheet | |
| 17 | Term Exams | Textbooks, Laboratory sheet |
Assessment (Exam) Methods and Criteria
| Assessment Type | Midterm / Year Impact | End of Term / End of Year Impact |
|---|---|---|
| 1. Midterm Exam | 40 | 16 |
| 1. Short Exam | 30 | 12 |
| 1. Performance Task (Laboratory) | 30 | 12 |
| General Assessment | ||
| Midterm / Year Total | 100 | 40 |
| 1. Final Exam | - | 60 |
| Grand Total | - | 100 |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 1 | 14 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 2 | 28 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 3 | 3 |
| Final Exam | 1 | 9 | 9 |
| Total Workload (Hour) | 54 | ||
| Total Workload / 25 (h) | 2,16 | ||
| ECTS | 2 ECTS | ||