TÜRKÇE
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Information
| Code | KM237 |
| Name | Organic Chemistry Lab. 1 |
| Term | 2022-2023 Academic Year |
| Semester | 3. Semester |
| Duration (T+A) | 0-4 (T-A) (17 Week) |
| ECTS | 3 ECTS |
| National Credit | 2 National Credit |
| Teaching Language | Türkçe |
| Level | Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Prof. Dr. ELİFE SULTAN GİRAY |
| Course Instructor |
Prof. Dr. ELİFE SULTAN GİRAY
(A Group)
(Ins. in Charge)
Öğr. Gör.Dr. ONUR DEMİRKOL (A Group) (Asst. Ins.) |
Course Goal / Objective
Understanding the basic purification methods and establishing some basic organic reaction mechanisms, obtaining the product, determining the structure by product purification and FTIR analysis
Course Content
The basic purification methods used in Organic Chemistry and applications of some organic reactions
Course Precondition
none
Resources
Experimental Organic Chemistry Ender Erdik
Notes
Organic Chemistry T. W. Graham Solomons, Craig B. Fryhle, Scott A. Snyder
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | Understands the solubility of different organic compounds in different solvents |
| LO02 | Separates different liquid mixtures from each other with distillation method, determines the amount of each, comments on which liquid it is. |
| LO03 | Understands the crystallization method, separates and determines different solids with this method. |
| LO04 | Understands the sublimation method, learns to use this method in separation processes |
| LO05 | Understands the extraction method, using this method, it can separate a painkiller tablet into its components. |
| LO06 | Understands chromatographic methods, separates and purifies different substances with this method |
| LO07 | Understand the structure determination of substances with FTIR spectroscopy |
| LO08 | Synthesizes n-butylbromide, learns the SN2 reaction mechanism, can purify the product and determine its structure. |
| LO09 | Synthesizes t-butylchloride, learns SN1 reaction mechanism, purifies the product and determines its structure. |
| LO10 | Syntheses 2-hexanol, learn how to eliminate mercury element, purify the product, determine its structure by FTIR analysis |
| LO11 | Perform halogenation experiment of alkanes, learn MSDS information of bromine element, comprehend halogenation reaction |
| LO12 | Synthesis Diisobutylene, purifies the product and determines its structure |
| LO13 | Performs Compensation Experiments. |
| LO14 | understands separation techniques and which separation technique should be used in which situation. |
| LO15 | Comprehends the environmental conditions required for the elimination and substitution reactions to take place. |
| LO16 | Understands the application of thin layer chromatography and column chromatography techniques |
| LO17 | Understands the necessary conditions for synthesis in a laboratory environment |
| LO18 | Comprehends how the product obtained at the end of the experiment should be purified using which separation technique. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Relates his/her knowledge in the field of chemistry to life and industry by relying on his/her knowledge | |
| PLO02 | Bilgi - Kuramsal, Olgusal | Evaluates the developments in the world by following and perceiving the orientations in the industry. | 3 |
| PLO03 | Bilgi - Kuramsal, Olgusal | Gains awareness of lifelong learning and renews his/her knowledge. | 2 |
| PLO04 | Bilgi - Kuramsal, Olgusal | Access to information and associate their knowledge with other fields of science. | 5 |
| PLO05 | Bilgi - Kuramsal, Olgusal | Understands the need to combine information in the application of information and perceives the total quality awareness. | |
| PLO06 | Bilgi - Kuramsal, Olgusal | S/he has knowledge in the use of resources, in the creation of technology depending on the country's resources. | 4 |
| PLO07 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | S/he conveys what s/he knows to people close or distant to the subject by concretising. | 3 |
| PLO08 | Yetkinlikler - Öğrenme Yetkinliği | Gains the ability to access new information and technology. | 5 |
| PLO09 | Bilgi - Kuramsal, Olgusal | Learns to think creatively and produce solutions to problems in the field. | 2 |
| PLO10 | Yetkinlikler - Öğrenme Yetkinliği | To be able to associate information by having the ability of reasoning and transfer what they know to practice. | 3 |
| PLO11 | Beceriler - Bilişsel, Uygulamalı | Sets up laboratory equipment and makes decisions alone. | 5 |
| PLO12 | Bilgi - Kuramsal, Olgusal | To be able to follow the current technology in the field of chemistry and gain added value. | 4 |
| PLO13 | Bilgi - Kuramsal, Olgusal | Follows the developments, gains the ability to follow the directions in the field. | 3 |
| PLO14 | Bilgi - Kuramsal, Olgusal | Knowing information sharing and participating in teamwork and directing the team. | 4 |
| PLO15 | Beceriler - Bilişsel, Uygulamalı | Gains universal thinking and critical perspective. | |
| PLO16 | Bilgi - Kuramsal, Olgusal | Starts to have a say in the field. | 5 |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Solubility Tests | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 2 | Distillation | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 3 | Crystallization | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 4 | Sublimation | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 5 | Extraction | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 6 | Chromatographic methods | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 7 | Structure determination with FTIR Spectroscopy | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 8 | Mid-Term Exam | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 9 | Synthesis of n-butylbromide | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 10 | Synthesis of t-butylcloride | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 11 | Synthesis of 2-hexanol | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 12 | Halogenation of alkanes | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 13 | Synthesis of diisobutylene | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 14 | Finding Rf by thin layer chromatography | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 15 | ompensating experiments | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 16 | Term Exams-1 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 17 | Term Exams-2 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 0 | 0 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 2 | 28 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 12 | 12 |
| Final Exam | 1 | 24 | 24 |
| Total Workload (Hour) | 64 | ||
| Total Workload / 25 (h) | 2,56 | ||
| ECTS | 3 ECTS | ||