KM236 Organic Chemistry Lab. 2

3 ECTS - 0-4 Duration (T+A)- 4. Semester- 2 National Credit

Information

Code KM236
Name Organic Chemistry Lab. 2
Semester 4. Semester
Duration (T+A) 0-4 (T-A) (17 Week)
ECTS 3 ECTS
National Credit 2 National Credit
Teaching Language Türkçe
Level Lisans Dersi
Type Normal
Mode of study Yüz Yüze Öğretim
Catalog Information Coordinator Prof. Dr. ELİFE SULTAN GİRAY


Course Goal

Understanding the basic purification methods and establishing some basic organic reaction mechanisms, obtaining the product, determining the structure by product purification and FTIR analysis

Course Content

The basic purification methods used in Organic Chemistry and applications of some organic reactions

Course Precondition

none

Resources

Experimental Organic Chemistry Ender Erdik

Notes

Organic Chemistry T. W. Graham Solomons, Craig B. Fryhle, Scott A. Snyder


Course Learning Outcomes

Order Course Learning Outcomes
LO01 m-dinitrobenzene synthesizes, purifies and determines its structure by FTIR spectroscopy
LO02 Synthesizes the 2,4-dinitro-1-naphthol compound, at the same time, comprehends both the sulfation and nitration reactions, purifies the product and illuminates its structure.
LO03 Synthesize p-benzoquinone, understand oxidation reactions, make product purification and structure determination
LO04 Synthesis Ethyl acetate, learns the esterification reactions, purifies the product and illuminates its structure
LO05 Synthesizes benzoin, learns condensation reactions, purifies the product and brightens its structure
LO06 Performs Compensation Experiments.
LO07 comprehend chromatographic methods.
LO08 Synthesize Coumarin compounds, learn condensation reactions, purify the product and brighten its structure
LO09 Synthesizes the chalcone compound, learns the condensation reactions, purifies the product and brightens its structure.
LO10 Can synthesize phthalimide, purifies the product and brightens its structure.
LO11 Can synthesize adipic acid, learn oxidation reactions, purify the product and brighten its structure
LO12 Can do dyestuff synthesis, learn coupling reactions, purify the product and brighten its structure
LO13 Comprehends the safety precautions to be applied while working in the laboratory.
LO14 Comprehends the safety and first aid information to be applied against the chemicals to be used in the experiments.
LO15 Understands and applies separation techniques
LO16 Learns to use glass materials necessary to set up experiments
LO17 Understands which separation technique should be used to separate the product obtained at the end of the experiment from the environment.
LO18 Understands and applies the rules to be followed while working in the laboratory
LO19 comprehend and apply purification techniques.
LO20 understands what to do in case of an accident in the laboratory.


Relation with Program Learning Outcome

Order Type Program Learning Outcomes Level
PLO01 Bilgi - Kuramsal, Olgusal Relates his/her knowledge in the field of chemistry to life and industry by relying on his/her knowledge 4
PLO02 Bilgi - Kuramsal, Olgusal Evaluates the developments in the world by following and perceiving the orientations in the industry. 3
PLO03 Bilgi - Kuramsal, Olgusal Gains awareness of lifelong learning and renews his/her knowledge.
PLO04 Bilgi - Kuramsal, Olgusal Access to information and associate their knowledge with other fields of science.
PLO05 Bilgi - Kuramsal, Olgusal Understands the need to combine information in the application of information and perceives the total quality awareness. 2
PLO06 Bilgi - Kuramsal, Olgusal S/he has knowledge in the use of resources, in the creation of technology depending on the country's resources. 2
PLO07 Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği S/he conveys what s/he knows to people close or distant to the subject by concretising.
PLO08 Yetkinlikler - Öğrenme Yetkinliği Gains the ability to access new information and technology. 3
PLO09 Bilgi - Kuramsal, Olgusal Learns to think creatively and produce solutions to problems in the field. 5
PLO10 Yetkinlikler - Öğrenme Yetkinliği To be able to associate information by having the ability of reasoning and transfer what they know to practice. 2
PLO11 Beceriler - Bilişsel, Uygulamalı Sets up laboratory equipment and makes decisions alone. 5
PLO12 Bilgi - Kuramsal, Olgusal To be able to follow the current technology in the field of chemistry and gain added value. 4
PLO13 Bilgi - Kuramsal, Olgusal Follows the developments, gains the ability to follow the directions in the field. 5
PLO14 Bilgi - Kuramsal, Olgusal Knowing information sharing and participating in teamwork and directing the team. 4
PLO15 Beceriler - Bilişsel, Uygulamalı Gains universal thinking and critical perspective. 4
PLO16 Bilgi - Kuramsal, Olgusal Starts to have a say in the field. 5


Week Plan

Week Topic Preparation Methods
1 Synthesis of m-dinitrobenzene Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
2 Synthesis of 2,4-dinitro-1-naphthol Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
3 Synthesis of p-benzoquinone Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
4 Synthesis of ethylacetate Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
5 Synthesis of benzoin Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
6 compensating experiments-1 Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
7 compensating experiments-2 Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
8 Mid-Term Exam Experimental Organic Chemistry Ender Erdik Ölçme Yöntemleri:
Yazılı Sınav
9 Synthesis of coumarin Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
10 Synthesis of chalcone Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
11 synthesis of phthalimide Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
12 Syntesis of adipic acid Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
13 dyestuff synthesis Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
14 compensating experiments-3 Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
15 compensating experiments-4 Experimental Organic Chemistry Ender Erdik Öğretim Yöntemleri:
Deney / Laboratuvar
16 Term Exams-1 Experimental Organic Chemistry Ender Erdik Ölçme Yöntemleri:
Yazılı Sınav
17 Term Exams-2 Experimental Organic Chemistry Ender Erdik Ölçme Yöntemleri:
Yazılı Sınav


Student Workload - ECTS

Works Number Time (Hour) Workload (Hour)
Course Related Works
Class Time (Exam weeks are excluded) 14 0 0
Out of Class Study (Preliminary Work, Practice) 14 2 28
Assesment Related Works
Homeworks, Projects, Others 0 0 0
Mid-term Exams (Written, Oral, etc.) 1 12 12
Final Exam 1 24 24
Total Workload (Hour) 64
Total Workload / 25 (h) 2,56
ECTS 3 ECTS