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Information
| Code | CMT0028 |
| Name | Technics of Materials Characterization |
| Term | 2022-2023 Academic Year |
| Semester | . Semester |
| Duration (T+A) | 3-0 (T-A) (17 Week) |
| ECTS | 6 ECTS |
| National Credit | 3 National Credit |
| Teaching Language | Türkçe |
| Level | Yüksek Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator |
Course Goal / Objective
It is aimed to introduce the main methods and tools/devices used in structural material characterization and to teach the examination and analysis of material structure and properties.
Course Content
Introduction to Materials Characterization, Methods of Materials Characterization, Material Preparation for Analysis, Matters Needing Attention for Material Preparation and Analysis, Material and Microstructural Geometry, Optical Microscope, Material Preparation for Optic Microscope and Method of Microstructural Analysis, SEM Analysis, Material Preparation for SEM, Microstructural-Morphological Analysis Method, Definition of XRF, Interpretation of Chemical Composition and Loss of Burning, Working Principle of X-Ray Diffraction (X-Ray) Device, Phase Analysis and Interpretation, Definition of DSC Method, Interpretation of Obtained Experimental Outcomes and Graphics, Definition of DTA-TGA Method, Interpretation of Obtained Experimental Outcomes and Graphics, Analysis and Interpretation of FTIR Analysis, Analysis and Interpretation of XPS Analysis, Analysis and Interpretation of AFM Analysis.
Course Precondition
There is no prerequsite for this course
Resources
Lecture notes
Notes
Lecture notes
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | Explains the principles of sample preparation in material characterization. |
| LO02 | Lists material characterization methods |
| LO03 | Analysis SEM/TEM images of materials in material chacterization. |
| LO04 | Knows what the peaks in XRD patterns of materials mean. |
| LO05 | Reads DTA/TGA curves of materials in thermal analysis |
| LO06 | Reads FTIR curves of materials |
| LO07 | Makes analysis of XRF of chemical composition of materials |
| LO08 | Explains importance of material characterization in industrial application |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Is dominated with basic concepts, theories and principles in mechanical engineering | 3 |
| PLO02 | Bilgi - Kuramsal, Olgusal | Is equipped with the basic knowledge of math, science and engineering | 3 |
| PLO03 | Bilgi - Kuramsal, Olgusal | Uses computers effectively, has the ability of computer-aided drafting, design, analysis, and presentation | 2 |
| PLO04 | Beceriler - Bilişsel, Uygulamalı | Plans and does experiments in advanced level, interpretes and analizes the results and the data | 4 |
| PLO05 | Beceriler - Bilişsel, Uygulamalı | Is equipped with a variety of skills and advanced engineering techniques | 4 |
| PLO06 | Beceriler - Bilişsel, Uygulamalı | To design a system, component or process in order to meet the needs of various engineering problems within the limitations of technical, economic, environmental, manufacturability, sustainability | |
| PLO07 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | Independently reviews and learns the applications in an enterprise, makes a critical assessment of the problems faced with, has the ability of selecting the proper technique to formulate problems and propose solutions | 3 |
| PLO08 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | Identifies a product or its production process, design, development, and prioritise its use | |
| PLO09 | Yetkinlikler - Öğrenme Yetkinliği | Becomes aware of the necessity of lifelong learning and continuously self-renew | |
| PLO10 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Is capable of effective oral and written English for technical or non-technical use | 3 |
| PLO11 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Has teamwork skills, good communication skills and works efficiently as a member of versatile and an interdisciplinary team | 3 |
| PLO12 | Yetkinlikler - Alana Özgü Yetkinlik | Is aware of the technical and ethical responsibilities, inquisitive and innovative | 4 |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Introduction to Material Characterization and basic and nanoscale material characterization methods | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 2 | Sample preparation principles in material characterization | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 3 | Sample etching technics in material characterization | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 4 | Mateial and microstructure geometry | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 5 | Fundamental Conceps on Light microscop and sample preparation | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 6 | Microstructural analysis in light microscopic examination | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 7 | SEM analysis and sample preparation for SEM analysis | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 8 | Mid-Term Exam | Writing exam | Ölçme Yöntemleri: Yazılı Sınav |
| 9 | IInvestigating microstructure-morphological analysis in SEM analysis | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 10 | XRD analysis and phase interpretation | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 11 | Rietveld method in XRD analysis | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 12 | XRF analysis, Chemical composition and loss of ignition | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 13 | Thermal analysis definition and fundamental concepts | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 14 | Thermal analysis methods | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 15 | IR analysis methods | The relevant section from the lecture notes should be read and internet research should be done. | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 16 | Term Exams | Writing exam | Ölçme Yöntemleri: Yazılı Sınav |
| 17 | Term Exams | Wriying exam | Yöntem Seçilmemiş |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 3 | 42 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 5 | 70 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 15 | 15 |
| Final Exam | 1 | 30 | 30 |
| Total Workload (Hour) | 157 | ||
| Total Workload / 25 (h) | 6,28 | ||
| ECTS | 6 ECTS | ||