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Information
| Code | KM002 |
| Name | Analysis of Organic Compounds with Spectroscopic Methods |
| Term | 2022-2023 Academic Year |
| Term | Spring |
| Duration (T+A) | 3-0 (T-A) (17 Week) |
| ECTS | 5 ECTS |
| National Credit | 3 National Credit |
| Teaching Language | Türkçe |
| Level | Yüksek Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Prof. Dr. ELİFE SULTAN GİRAY |
| Course Instructor |
1 |
Course Goal / Objective
teaching identification of structure of organic compounds bymolecular spectroscopic methods
Course Content
Using IR, 13C NMR, 1H NMR andMSmethodsfor identification of organic compounds
Course Precondition
none
Resources
Spectrometric Identification of Organic Compounds Robert M. Silverstein , Francis X. Webster, David J. Kiemle
Notes
Spectroscopic Methods in Organic Chemistry Hesse–Meier–Zeeh, Thieme
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | students learn how to illuminate the structure of organic compounds using spectroscopic techniques |
| LO02 | Learn the applications of mass spectroscopy |
| LO03 | Determine the molecular structure by mass spectroscopy |
| LO04 | Students learn the investigation of molecules with NMR |
| LO05 | Students learn the investigation of molecules with IR |
| LO06 | Students learn the investigation of molecules with MS supported NMR and IR methods |
| LO07 | Learn the solution of combined spectroscopic problems |
| LO08 | learn the determination of formula of unknown molecules |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Reaches, evaluates and interprets information by doing research in the field of chemistry. | 4 |
| PLO02 | Bilgi - Kuramsal, Olgusal | S/he has extensive knowledge of the techniques and methods applied in the field of chemistry. | 3 |
| PLO03 | Bilgi - Kuramsal, Olgusal | Becomes aware of new and developing applications in the field, gains the competence to examine, learn and apply. | 2 |
| PLO04 | Bilgi - Kuramsal, Olgusal | Designs institutional modeling and empirical research and solves the problems encountered. | 4 |
| PLO05 | Bilgi - Kuramsal, Olgusal | Follows scientific developments in her/his field. | 4 |
| PLO06 | Bilgi - Kuramsal, Olgusal | Plans and maintains a scientific study. | |
| PLO07 | Bilgi - Kuramsal, Olgusal | Gains the ability to adapt to new situations and solve problems. | |
| PLO08 | Bilgi - Kuramsal, Olgusal | Reaches new technology in the field. | 3 |
| PLO09 | Bilgi - Kuramsal, Olgusal | Gains the ability to work independently and in teams and to take responsibility in the field. | |
| PLO10 | Beceriler - Bilişsel, Uygulamalı | Follows the directions in the field, gains the ability to solve complex situations. | 3 |
| PLO11 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | Presents the results of their studies in written and oral form. Approaches environmental problems scientifically. | |
| PLO12 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | It observes scientific and ethical values in the stages of data collection, interpretation and announcement. | 4 |
| PLO13 | Yetkinlikler - Öğrenme Yetkinliği | It produces solutions by making scientific approaches to the problems related to living spaces and conditions, and raises awareness by informing the environment. | 5 |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | What is spectroscopy and molecular spectroskopy | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 2 | How to determine the structure withmassspectroscopic method | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 3 | Examples on the structure determination byMassspectroscopic method | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 4 | Structure identification by mass spectroscopic method | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 5 | How to determine the structure by NMR spectroscopic method | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 6 | Examples on the structure determination by NMR methods | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 7 | Examples on the structure determination by Mass and NMR spectroscopic method | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 8 | Mid-Term Exam | studying from textbook and benefits of internet | Ölçme Yöntemleri: Yazılı Sınav, Ödev |
| 9 | Structure determination by mass spectroscopic method and IR spectroscopic method | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 10 | Examples on structure determination by mass spectroscopic method and IR spectroscopic method | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 11 | Examples on the structure determination by IR spectrometry | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 12 | Defining the molecular structure using by all three methods | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 13 | Molecular structure identification using different spectroscopic methods | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 14 | Examples on molecular structure identification using different spectroscopic methods | studying from textbook and benefits of internet | Öğretim Yöntemleri: Soru-Cevap, Anlatım, Tartışma, Alıştırma ve Uygulama |
| 15 | Examples on molecular structure identification using all three methods | studying from textbook and benefits of internet | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama |
| 16 | General topic repetition with question solutions | studying from textbook and benefits of internet | Öğretim Yöntemleri: Soru-Cevap, Alıştırma ve Uygulama |
| 17 | Term Exams | studying from textbook and benefits of internet | Ölçme Yöntemleri: Yazılı Sınav, Ödev |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 3 | 42 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 3 | 42 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 12 | 12 |
| Final Exam | 1 | 18 | 18 |
| Total Workload (Hour) | 114 | ||
| Total Workload / 25 (h) | 4,56 | ||
| ECTS | 5 ECTS | ||