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Information
| Code | KM237 |
| Name | Organic Chemistry Lab. 1 |
| Term | 2024-2025 Academic Year |
| Semester | 3. Semester |
| Duration (T+A) | 0-4 (T-A) (17 Week) |
| ECTS | 3 ECTS |
| National Credit | 2 National Credit |
| Teaching Language | Türkçe |
| Level | Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Prof. Dr. ELİFE SULTAN GİRAY |
| Course Instructor |
Prof. Dr. ELİFE SULTAN GİRAY
(A Group)
(Ins. in Charge)
|
Course Goal / Objective
The aim of this course is to understand the basic purification methods and to establish some basic organic reaction mechanisms, to obtain the product, to purify the product and to determine its structure by FTIR analysis.
Course Content
In this course, basic purification methods and applications of some organic reactions that are frequently used in organic chemistry are covered.
Course Precondition
none
Resources
Experimental Organic Chemistry Ender Erdik
Notes
Organic Chemistry T. W. Graham Solomons, Craig B. Fryhle, Scott A. Snyder
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | Classifies the solubility of different organic compounds in different solvents. |
| LO02 | Separates different liquid mixtures from each other with distillation method, determines the amount of each, comments on which liquid it is. |
| LO03 | Understands the crystallization method, separates and determines different solids with this method. |
| LO04 | Understands the sublimation method and relates to using this method in separation processes. |
| LO05 | Describes the extraction method, using this method, it can separate a painkiller tablet into its components. |
| LO06 | Describes chromatographic methods, separates and purifies different substances with this method |
| LO07 | Defines the structure determination of substances by FTIR spectroscopy. |
| LO08 | Synthesizes n-butylbromide, learns the SN2 reaction mechanism, can purify the product and determine its structure. |
| LO09 | Synthesizes t-butylchloride, learns SN1 reaction mechanism, purifies the product and determines its structure. |
| LO10 | Syntheses 2-hexanol, learn how to eliminate mercury element, purify the product, determine its structure by FTIR analysis |
| LO11 | Performs the halogenation experiment of alkanes, learns the MSDS information of the bromine element, and relates the halogenation reaction. |
| LO12 | Synthesis Diisobutylene, purifies the product and determines its structure |
| LO13 | Performs Compensation Experiments. |
| LO14 | Determines the separation techniques and which separation technique should be used in which situation. |
| LO15 | Determines the environmental conditions required for the elimination and substitution reactions to take place. |
| LO16 | Relates the application of thin layer chromatography and column chromatography techniques. |
| LO17 | Determines the conditions required for synthesis in the laboratory environment. |
| LO18 | Determines how the product obtained at the end of the experiment should be purified using which separation technique. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Relates his/her knowledge in the field of chemistry to life and industry by relying on his/her knowledge | |
| PLO02 | Bilgi - Kuramsal, Olgusal | Evaluates the developments in the world by following and perceiving the orientations in the industry. | 3 |
| PLO03 | Bilgi - Kuramsal, Olgusal | Gains awareness of lifelong learning and renews his/her knowledge. | 2 |
| PLO04 | Bilgi - Kuramsal, Olgusal | Access to information and associate their knowledge with other fields of science. | 3 |
| PLO05 | Bilgi - Kuramsal, Olgusal | Understands the need to combine information in the application of information and perceives the total quality awareness. | |
| PLO06 | Bilgi - Kuramsal, Olgusal | S/he has knowledge in the use of resources, in the creation of technology depending on the country's resources. | 2 |
| PLO07 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | S/he conveys what s/he knows to people close or distant to the subject by concretising. | 3 |
| PLO08 | Yetkinlikler - Öğrenme Yetkinliği | Gains the ability to access new information and technology. | 3 |
| PLO09 | Bilgi - Kuramsal, Olgusal | Learns to think creatively and produce solutions to problems in the field. | 2 |
| PLO10 | Yetkinlikler - Öğrenme Yetkinliği | To be able to associate information by having the ability of reasoning and transfer what they know to practice. | 3 |
| PLO11 | Beceriler - Bilişsel, Uygulamalı | Sets up laboratory equipment and makes decisions alone. | 3 |
| PLO12 | Bilgi - Kuramsal, Olgusal | To be able to follow the current technology in the field of chemistry and gain added value. | 2 |
| PLO13 | Bilgi - Kuramsal, Olgusal | Follows the developments, gains the ability to follow the directions in the field. | 3 |
| PLO14 | Bilgi - Kuramsal, Olgusal | Knowing information sharing and participating in teamwork and directing the team. | 4 |
| PLO15 | Beceriler - Bilişsel, Uygulamalı | Gains universal thinking and critical perspective. | |
| PLO16 | Bilgi - Kuramsal, Olgusal | Starts to have a say in the field. | 4 |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Solubility Tests | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Alıştırma ve Uygulama, Soru-Cevap |
| 2 | Distillation | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Soru-Cevap, Tartışma |
| 3 | Crystallization | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Soru-Cevap, Tartışma |
| 4 | Sublimation | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Soru-Cevap, Tartışma |
| 5 | Extraction | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 6 | Chromatographic methods | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 7 | Structure determination with FTIR Spectroscopy | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Soru-Cevap, Tartışma |
| 8 | Mid-Term Exam | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 9 | Synthesis of n-butylbromide | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 10 | Synthesis of t-butylcloride | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 11 | Synthesis of 2-hexanol | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 12 | Halogenation of alkanes | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Soru-Cevap, Tartışma |
| 13 | Synthesis of diisobutylene | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 14 | Finding Rf by thin layer chromatography | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 15 | ompensating experiments | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 16 | Term Exams-1 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 17 | Term Exams-2 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 0 | 0 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 2 | 28 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 12 | 12 |
| Final Exam | 1 | 24 | 24 |
| Total Workload (Hour) | 64 | ||
| Total Workload / 25 (h) | 2,56 | ||
| ECTS | 3 ECTS | ||