TÜRKÇE
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Information
| Code | KM236 |
| Name | Organic Chemistry Lab. 2 |
| Term | 2024-2025 Academic Year |
| Semester | 4. Semester |
| Duration (T+A) | 0-4 (T-A) (17 Week) |
| ECTS | 3 ECTS |
| National Credit | 2 National Credit |
| Teaching Language | Türkçe |
| Level | Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Prof. Dr. ELİFE SULTAN GİRAY |
| Course Instructor |
1 2 Öğr. Gör.Dr. ONUR DEMİRKOL (A Group) (Asst. Ins.) |
Course Goal / Objective
The aim of this course is to understand the basic purification methods and to establish some basic organic reaction mechanisms, to obtain the product, to purify the product and to determine its structure by FTIR analysis.
Course Content
In this course, basic purification methods and applications of some organic reactions that are frequently used in organic chemistry are covered.
Course Precondition
none
Resources
Experimental Organic Chemistry Ender Erdik
Notes
Organic Chemistry T. W. Graham Solomons, Craig B. Fryhle, Scott A. Snyder
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | m-dinitrobenzene synthesizes, purifies and determines its structure by FTIR spectroscopy |
| LO02 | Synthesizes the 2,4-dinitro-1-naphthol compound, at the same time, comprehends both the sulfation and nitration reactions, purifies the product and illuminates its structure. |
| LO03 | Synthesize p-benzoquinone, determine oxidation reactions, make product purification and structure determination |
| LO04 | Synthesis Ethyl acetate, learns the esterification reactions, purifies the product and illuminates its structure |
| LO05 | Synthesizes benzoin, learns condensation reactions, purifies the product and brightens its structure |
| LO06 | Performs Compensation Experiments. |
| LO07 | determine chromatographic methods. |
| LO08 | Synthesize Coumarin compounds, learn condensation reactions, purify the product and brighten its structure |
| LO09 | Synthesizes the chalcone compound, learns the condensation reactions, purifies the product and brightens its structure. |
| LO10 | Can synthesize phthalimide, purifies the product and brightens its structure. |
| LO11 | Can synthesize adipic acid, learn oxidation reactions, purify the product and brighten its structure |
| LO12 | Can do dyestuff synthesis, learn coupling reactions, purify the product and brighten its structure |
| LO13 | Determines the safety precautions to be applied while working in the laboratory. |
| LO14 | Determines the safety and first aid information to be applied against the chemicals to be used in the experiments. |
| LO15 | Determines and applies separation techniques |
| LO16 | Learns to use glass materials necessary to set up experiments |
| LO17 | Determines which separation technique should be used to separate the product obtained at the end of the experiment from the environment. |
| LO18 | Determines and applies the rules to be followed while working in the laboratory |
| LO19 | Determines and apply purification techniques. |
| LO20 | Determines what to do in case of an accident in the laboratory. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Relates his/her knowledge in the field of chemistry to life and industry by relying on his/her knowledge | 3 |
| PLO02 | Bilgi - Kuramsal, Olgusal | Evaluates the developments in the world by following and perceiving the orientations in the industry. | 3 |
| PLO03 | Bilgi - Kuramsal, Olgusal | Gains awareness of lifelong learning and renews his/her knowledge. | |
| PLO04 | Bilgi - Kuramsal, Olgusal | Access to information and associate their knowledge with other fields of science. | |
| PLO05 | Bilgi - Kuramsal, Olgusal | Understands the need to combine information in the application of information and perceives the total quality awareness. | |
| PLO06 | Bilgi - Kuramsal, Olgusal | S/he has knowledge in the use of resources, in the creation of technology depending on the country's resources. | |
| PLO07 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | S/he conveys what s/he knows to people close or distant to the subject by concretising. | |
| PLO08 | Yetkinlikler - Öğrenme Yetkinliği | Gains the ability to access new information and technology. | 3 |
| PLO09 | Bilgi - Kuramsal, Olgusal | Learns to think creatively and produce solutions to problems in the field. | 3 |
| PLO10 | Yetkinlikler - Öğrenme Yetkinliği | To be able to associate information by having the ability of reasoning and transfer what they know to practice. | |
| PLO11 | Beceriler - Bilişsel, Uygulamalı | Sets up laboratory equipment and makes decisions alone. | 3 |
| PLO12 | Bilgi - Kuramsal, Olgusal | To be able to follow the current technology in the field of chemistry and gain added value. | 3 |
| PLO13 | Bilgi - Kuramsal, Olgusal | Follows the developments, gains the ability to follow the directions in the field. | 4 |
| PLO14 | Bilgi - Kuramsal, Olgusal | Knowing information sharing and participating in teamwork and directing the team. | |
| PLO15 | Beceriler - Bilişsel, Uygulamalı | Gains universal thinking and critical perspective. | 3 |
| PLO16 | Bilgi - Kuramsal, Olgusal | Starts to have a say in the field. | 4 |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Synthesis of m-dinitrobenzene | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 2 | Synthesis of 2,4-dinitro-1-naphthol | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Soru-Cevap, Grup Çalışması |
| 3 | Synthesis of p-benzoquinone | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 4 | Synthesis of ethylacetate | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 5 | Synthesis of benzoin | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 6 | compensating experiments-1 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 7 | compensating experiments-2 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 8 | Mid-Term Exam | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 9 | Synthesis of coumarin | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 10 | Synthesis of chalcone | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 11 | synthesis of phthalimide | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 12 | Syntesis of adipic acid | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 13 | dyestuff synthesis | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 14 | compensating experiments-3 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 15 | compensating experiments-4 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar, Grup Çalışması, Soru-Cevap |
| 16 | Term Exams-1 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 17 | Term Exams-2 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 0 | 0 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 2 | 28 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 12 | 12 |
| Final Exam | 1 | 24 | 24 |
| Total Workload (Hour) | 64 | ||
| Total Workload / 25 (h) | 2,56 | ||
| ECTS | 3 ECTS | ||